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AZEO-SEP™ (Pervaporation)hybrid units can be utilized in conjunction with conventional distillation columns. A portion of the overhead product from the column passes through the AZEO-SEP™ (Pervaporation)modules. In doing so, the azeotrope is broken and a pure product is produced. The permeate is returned to the column. This process is used to debottleneck the overall dehydration process by achieving the desired level of separation.